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排序方式: 共有6014条查询结果,搜索用时 15 毫秒
51.
《Journal of separation science》2017,40(21):4256-4263
Polypyrrole‐magnetite dispersive micro‐solid‐phase extraction method combined with ultraviolet‐visible spectrophotometry was developed for the determination of selected cationic dyes in textile wastewater. Polypyrrole‐magnetite was used as adsorbent due to its thermal stability, magnetic properties, and ability to adsorb Rhodamine 6G and crystal violet. Dispersive micro‐solid‐phase extraction parameters were optimized, including sample pH, adsorbent amount, extraction time, and desorption solvent. The optimum polypyrrole‐magnetite dispersive micro‐solid phase‐extraction conditions were sample pH 8, 60 mg polypyrrole‐magnetite adsorbent, 5 min of extraction time, and acetonitrile as the desorption solvent. Under the optimized conditions, the polypyrrole‐magnetite dispersive micro‐solid‐phase extraction with ultraviolet‐visible method showed good linearity in the range of 0.05–7 mg/L (R 2 > 0.9980). The method also showed a good limit of detection for the dyes (0.05 mg/L) and good analyte recoveries (97.4–111.3%) with relative standard deviations < 10%. The method was successfully applied to the analysis of dyes in textile wastewater samples where the concentration found was 1.03 mg (RSD ±7.9%) and 1.13 mg/L (RSD ± 4.6%) for Rhodamine 6G and crystal violet, respectively. It can be concluded that this method can be adopted for the rapid extraction and determination of dyes at trace concentration levels. 相似文献
52.
Nazl Turan Yücel Ümmühan Kandemir Ümide Demir
zkay
zgür Devrim Can 《Molecules (Basel, Switzerland)》2021,26(11)
Vortioxetine is a multimodal antidepressant drug that affects several brain neurochemicals and has the potential to induce various pharmacological effects on the central nervous system. Therefore, we investigated the centrally mediated analgesic efficacy of this drug and the mechanisms underlying this effect. Analgesic activity of vortioxetine (5, 10 and 20 mg/kg, p.o.) was examined by tail-clip, tail-immersion and hot-plate tests. Motor performance of animals was evaluated using Rota-rod device. Time course measurements (30–180 min) showed that vortioxetine (10 and 20 mg/kg) administrations significantly increased the response latency, percent maximum possible effect and area under the curve values in all of the nociceptive tests. These data pointed out the analgesic effect of vortioxetine on central pathways carrying acute thermal and mechanical nociceptive stimuli. Vortioxetine did not alter the motor coordination of mice indicating that the analgesic activity of this drug was specific. In mechanistic studies, pre-treatments with p-chlorophenylalanine (serotonin-synthesis inhibitor), NAN-190 (serotonin 5-HT1A receptor antagonist), α-methyl-para-tyrosine (catecholamine-synthesis inhibitor), phentolamine (non-selective α-adrenoceptor blocker), and naloxone (non-selective opioid receptor blocker) antagonised the vortioxetine-induced analgesia. Obtained findings indicated that vortioxetine-induced analgesia is mediated by 5-HT1A serotonergic, α-adrenergic and opioidergic receptors, and contributions of central serotonergic and catecholaminergic neurotransmissions are critical for this effect. 相似文献
53.
Egor A. Kapitonov Natalia N. Petrova Vasilii V. Mukhin Leonid A. Nikiforov Vladimir D. Gogolev Ee Le Shim Aitalina A. Okhlopkova Jin-Ho Cho 《Molecules (Basel, Switzerland)》2021,26(4)
The physical and mechanical properties of nitrile–butadiene rubber (NBR) composites with N-cetylpyridinium bromide-carbon black (CPB-CB) were investigated. Addition of 5 parts per hundred rubber (phr) of CPB-CB into NBR improved the tensile strength by 124%, vulcanization rate by 41%, shore hardness by 15%, and decreased the volumetric wear by 7% compared to those of the base rubber-CB composite. 相似文献
54.
The benefits of natural honeybee products (e.g., honey, royal jelly, beeswax, propolis, beevenom and pollen) to the immune system are remarkable, and many of them are involved in the induction of antibody production, maturation of immune cells and stimulation of the immune system. The type of plants in the geographical area, climatic conditions and production method have a significantly influence on the nutritional quality of honey. However, this variability can influence consumer liking by the sensory attributes of the product. The aim of this work was to compare the most popular honeys from Poland in terms of nutritional value, organoleptic properties and antioxidant activity. In the study, five varieties of honey (honeydew, forest, buckwheat, linden and dandelion) from conventional and organic production methods were tested. The nutritional characteristics of honey samples included acidity, content of water, sugars, vitamin C, HMF and phenolics (total and flavonoids), while honey color, taste, aroma and consistency were investigated in the organoleptic characteristics. The antioxidant activity was determined in water- and ethanol-soluble honey extracts using DPPH and ORAC tests. The results showed that organoleptic and nutritional characteristics of popular Polish honeys differ significantly in relation to plant source and production method. The significant effect of honey variety on the content of HMF, saccharose and phenolics, as well as acidity and antioxidant capacity were noted. The impact of variety and variety × production method interaction was significant in the case of the content of vitamin C, glucose and fructose. A visible difference of buckwheat and forest honeys from other samples was observed. The highest content of total phenolics with antioxidant activity based on the SET mechanism was found in buckwheat honeys, while forest honeys were richer in flavonoids. 相似文献
55.
Dr. Atena B. Solea Dr. Christophe Curty Prof. Dr. Katharina M. Fromm Prof. Dr. Christophe Allemann Prof. Dr. Olimpia Mamula Steiner 《Chemistry (Weinheim an der Bergstrasse, Germany)》2022,28(55):e202201772
The toxicity of phosgene (COCl2) combined with its extensive use as a reactant and building block in the chemical industry make its fast and accurate detection a prerequisite. We have developed a carboxylic derivative of 5,6-pinenepyridine which is able to act as colorimetric and fluorimetric sensor for phosgene in air and solution. For the first time, the formation of a pyrido-[2,1-a]isoindolone was used for this purpose. In solution, the sensing reaction is extremely fast (under 5 s), selective and highly sensitive, with a limit of detection (LOD) of 9.7 nM/0.8 ppb. When fixed on a solid support, the sensor is able to detect the presence of gaseous phosgene down to concentrations of 0.1 ppm, one of the lowest values reported to date. 相似文献
56.
57.
杭州大剧院风压分布的风洞试验研究 总被引:4,自引:0,他引:4
杭州大剧院外观造型新颖独特,由一个近似为椭球的双曲面屋盖和一个倒置的圆锥面玻璃幕墙相交形成大剧院的主体建筑的外轮廓.本文结合该主体结构的抗风设计要求,制作了1:200刚性模型进行结构表面脉动风压平均风压分布的风洞试验研究,详细介绍了风洞试验及数据处理方法,讨论了在不同风向角下椭球面屋盖和圆锥面玻璃幕墙的风压分布.为了便于整体结构设计,本文根据结构的实际情况对椭球面和圆锥面进行分块并给出相应的分块风压数据,最后根据各风向角下的风压分布特征给出了整体结构抗风设计的最不利风向角. 相似文献
58.
静电力平衡式微型硅加速度计方案分析 总被引:5,自引:0,他引:5
静电力平衡式微型硅加速度计是一种新型加速度计。本文对这种加速度计的3种典型方案进行了分析,导出静电力(力矩)、静电力平衡回路刚度(角刚度)及加速度测量范围的表达式。有关结果可为这种加速度计参数设计提供理论依据。 相似文献
59.
惯性系统三轴综合测试转台总体设计若干问题的探讨 总被引:3,自引:0,他引:3
本文从框架形式、总体布局、轴承的种类和布置方式等方面,讨论了惯性系统三轴综合测试转台总体设计中的若干问题,从设计、制造和使用等方面阐述了各种总体布局形式的优缺点,并提出了自己的相应看法,最后讨论了目前惯导测试设备研究领域需要研究的关键技术。 相似文献
60.
In this paper, we propose a new prototype model of a micro pump using ICPF (Ionic Conducting Polymer Film) actuator as the
servo actuator. This micro pump consists of two active oneway valves that make use of the same ICPF actuator. The overall
size of this micro pump prototype is 12mm in diameter and 20 mm in length. The actuating mechanism is as follows: (1) The
ICPF actuator as the diaphragm is bent into anode side by application of electricity. Then the volume of the pump chamber
increases, resulting in the inflow of liquid from the inlet to the chamber. (2) By changing the current direction, the volume
of the pump chamber decreases, resulting in the liquid flow from the chamber to the outlet. (3) The ICPF actuator is put on
a sine voltage, the micro pump provides liquid flow from the inlet to the outlet continuously. Characteristic of the micro
pump is measured. The experimental results indicate that the micro pump has the satisfactory responses. 相似文献